Percent Transmittance 100- 80- 60- 40- 20- 0- 4000 3600 3200 2800 2400 H H CO₂H CO₂H 2000 1800 1600 1400 1200 1000 800 600

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter7: Components Of Optical Instruments
Section: Chapter Questions
Problem 7.16QAP
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Percent Transmittance
100
80-
60-
40-
20-
0+
4000
10
Yummi
H
H
CO₂H
CO₂H
3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 600
Wavenumber in cm-1
1
11.90 ppm
9
H
H
CO₂H
CO₂H
6
TEXT
1.34 ppm
5
8, ppm
4
H₂O
CD₂SOCD₂H
3
Transcribed Image Text:Percent Transmittance 100 80- 60- 40- 20- 0+ 4000 10 Yummi H H CO₂H CO₂H 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 600 Wavenumber in cm-1 1 11.90 ppm 9 H H CO₂H CO₂H 6 TEXT 1.34 ppm 5 8, ppm 4 H₂O CD₂SOCD₂H 3
2. The following IR and NMR were obtained for Alicia's Intermediate product,
anhydride, and the final product,
acid.
Bicyclo
Bicyclo
[2.2.1]hept-5-ene-2,3-dicarboxylic
[2.2.1]hept-5-ene-2,3-dicarboxylic
a. Interpret the three major signals from the IR spectrum.
b. Label all hydrogens with the data from ¹H NMR
c. Label all carbons with the provided data from ¹³C NMR.
Transcribed Image Text:2. The following IR and NMR were obtained for Alicia's Intermediate product, anhydride, and the final product, acid. Bicyclo Bicyclo [2.2.1]hept-5-ene-2,3-dicarboxylic [2.2.1]hept-5-ene-2,3-dicarboxylic a. Interpret the three major signals from the IR spectrum. b. Label all hydrogens with the data from ¹H NMR c. Label all carbons with the provided data from ¹³C NMR.
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