for 20 minutes. Then return, put it down, and weigh yourself immediately three times. Since reporting your weight is a little too personal, I want you to tell me the variation between each reading (called a first derivative measurement). You should see the first weight is somewhat higher than the rest; often as much as 2-3 pounds. What do you th. this tells you about your scale's quality? All other data is provided in the lab procedure Questions So, go ahead and answer them, then. a For measuring the block, (part 1) measure something and tell me what it is. Today, definitions. Here are your lab questions: 1. Define significant figure 2. Define accuracy 3. Define precision 4. How many significant figures are present in the measurement 0.053402 mm? How many are in 0.053400? Calculate the following: For three replicate (repeated) measurements, your values are as follows: 3.510 g; 3.565 g; 3.593 Answer the following questions: a. What is the average? b. the percentage error (the accepted value is 3.62 g) C. There is a±5% error in the accuracy; is the label mass true.

for 20 minutes. Then return, put it down, and weigh yourself immediately three times. Since reporting your weight is a little too personal, I want you to tell me the variation between each reading (called a first derivative measurement). You should see the first weight is somewhat higher than the rest; often as much as 2-3 pounds. What do you th. this tells you about your scale's quality? All other data is provided in the lab procedure Questions So, go ahead and answer them, then. a For measuring the block, (part 1) measure something and tell me what it is. Today, definitions. Here are your lab questions: 1. Define significant figure 2. Define accuracy 3. Define precision 4. How many significant figures are present in the measurement 0.053402 mm? How many are in 0.053400? Calculate the following: For three replicate (repeated) measurements, your values are as follows: 3.510 g; 3.565 g; 3.593 Answer the following questions: a. What is the average? b. the percentage error (the accepted value is 3.62 g) C. There is a±5% error in the accuracy; is the label mass true.

Appl Of Ms Excel In Analytical Chemistry

2nd Edition

ISBN:9781285686691

Author:Crouch

Publisher:Crouch

Chapter14: Chromatography

Section: Chapter Questions

Problem 9P

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Often the analyst will compare known quantities of analyte to unknown quantities of the material to be analyzed. This may be done in one of three ways: -use calibration curves; use standard additions; or use internal standards. The method of standard additions would be used when A) the quantity of sample analyzed or the instrument response varies from run to run. B) the standard solutions and the unknown solution all have similar characteristics are unaffected by the other material in the sample. C) the sample composition is unknown or complex and affects the analytical signal.
10) The following results were obtained in an analysis of iron content in an ore sample. The results reported as % Fe for each analysis, were as follow: Samples no. 1 3 4 5 6 % Fe 20.10 20.50 18.65 19.25 19.40 19.99 i. Calculate the mean and median from the set of the data above ii. If the true value of %Fe is 19.65 %, calculate the value for absolute error and percentage relative error for sample no. 3 Using Q-test, justify whether an of the data must be rejected at 95 % ii. confidence level iv. Calculate the standard deviation and relative standard deviation of the data.
Categorize each as a determinate or an indeterminate error and further classify determinate errors as instrumental, method or personal. a) An unknown sample being weighed is hygroscopic. b) One component of a mixture being analyzed quantitatively by GC reacts with the column packing. c) A radioactive sample being counted repeatedly without any change in condition yields a slightly different count at each trial. d) The tip of the pipet used in the analysis is broken. e) In measuring the same peak heights of a chromatogram, two technician each report different heights.
Find the mean and median of each of the following sets of data. Determine the deviation from the mean for each data point within the seats and find the mean deviation for each set. Use a spreadsheet if it is convenient. (a) 0.0110 0.0104. 0.0105
1. Research on the limitation of accuracy of the following instruments: • analytical balance • top-loading balance • serological pipette • graduated cylinder • burette • volumetric flask • Erlenmeyer flask • beaker 2. Define the term, "measurement uncertainty". Among the instruments listed above, which ones have the highest uncertainty? Which ones have the lowest? 3. Based on the measurement uncertainty of the above instruments, which instruments would yield the lowest percent error?
ESF X empt/quiz_start_frame_auto.d21?ou=9739790&isprv=&qi=11007766&cfql=0&dnb=0&fromQB=0&inProgress=1 ystems Question 5 (1 point) Ben starts walking along a path at 3 mi hr¹. Amanda starts jogging along the same path 1 hour later at 5 mi hr. After how much time jogging does Amanda catch up to Ben? 3.5 hr 2.5 hr 2 hr 16
[References) A method for the determination of the corticosteroid methylprednisolone acetate in solutions obtained from pharmaceutical preparations yielded a mean value of 3.7 mg mL with a standard deviation of 0.3 mg mL. For quality control purposes, the relative uncertainty in the concentration should be no more than 3%. How many samples of each batch should be analyzed to ensure that the relative standard deviation does not exceed 9% at the 95% confidence level? samples
I have trouble finding the answer and would really appreciate some help, pls explain and make sure its 1000% correct, thanks !!
Mission 2: Experiment- Tools and Techniques in Analytical Measurements Datasheet for 37 A-1: Using the Analytical Balance Measurement (s) Weight of Penny (g) [by Method 1] Weight of Penny (g) [by Method 2] Penny 1 2.48 2.51 Penny 2 2.49 2.50 Penny 3 2.50 2.52 2.49 2.48 Penny 4 Penny 5 2.51 2.47 From the above data, you will determine the mean and median values, the standard deviation, and the relative standard deviation of the masses of the pennies.
ASSAY Calibration solutions Calibration solutions of naproxen in the range 5 – 25 μg/mL were prepared. Sample preparation 20 tablets weighing 12.3819 g were crushed to a fine powder. A portion of the powder (145.4 mg) was shaken with approximately 150 mL of acetic acid (0.05 M) for 5 min and then made up to volume in a 250 mL volumetric flask (stock solution). Approximately 50 mL of the stock solution was filtered and a 25 mL aliquot was diluted to 100 mL in a volumetric flask. 10 mL of the resulting solution was further diluted to 100 mL with acetic acid (0.05 M). Analysis The standards and sample solutions were analyzed by HPLC under the following conditions: Column: octadecylsilyl (ODS), 4.6 mmx150 mm, mobile phase: acetonitrile : 0.05 M acetic acid (85:15), flow rate: 1 ml/min, UV detection at 243 nm. Results: A calibration curve of concentration versus peak area was constructed for the standard solutions and gave the straight-line equation: y = 3555.6x + 85, r = 0.9999 The area…
2) As an example of precision and accuracy of data, suppose the % carbon in a single compound has been measured thrce separate times by 2 different students. The theoretical % carbon is 21.34%. Student 1: trial 1:26.11%, trial 2: 26.24% trial 3: 25.92 %, Avg - 26.09 Student 2: trial 1: 20.35%. trial 2: 22.64 % trial 3: 19.79 %. Avg = 20.93 a) Which student had the more precise data and how can you tell? b) Which student had the more accurate data and how can you tell? 3a) Calculate the % error of Student 1 data in problem 2 above. Show all work below. WATCH SIG FIGS
Trial I Trial II Final reading HCI 26. 40 ml 27.10 ml Initial reading HCI 1.2 ml 1.8 ml Volume of HCl used ? ? Final reading NaOH 33.7 ml 32.8 ml Initial reading NaOH 0.8 mL 0.5 ml Volume of NaOH used ? ? For trial I: Normality of NaOH : 0.25 N Vol. of HCl used = final volume - initial volume Solve for the average Normality of HCI : ? NHCI x VHCI = NNAOH x VNAOH Vol. of NaOH used = final volume - initial volume NNAOH x VNAOH For trial II: NHCI = Vol. of HCl used = final volume - initial volume VHCI Activa Vol. of NaOH used = final volume - initial volume Go to S